Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Long-Term Bonding Performance of One-Bottle vs. Two-Bottle Bonding Agents to Lithium Disilicate Ceramics

Version 1 : Received: 9 July 2024 / Approved: 9 July 2024 / Online: 9 July 2024 (13:22:46 CEST)

How to cite: Irie, M.; Okada, M.; Maruo, Y.; Nishigawa, G.; Matsumoto, T. Long-Term Bonding Performance of One-Bottle vs. Two-Bottle Bonding Agents to Lithium Disilicate Ceramics. Preprints 2024, 2024070737. https://doi.org/10.20944/preprints202407.0737.v1 Irie, M.; Okada, M.; Maruo, Y.; Nishigawa, G.; Matsumoto, T. Long-Term Bonding Performance of One-Bottle vs. Two-Bottle Bonding Agents to Lithium Disilicate Ceramics. Preprints 2024, 2024070737. https://doi.org/10.20944/preprints202407.0737.v1

Abstract

Objective: The effect of long-term performance of one-bottle or two-bottle bonding agents on the shear bond strength to lithium disilicate ceramics (LDS) were to investigate, and the long-term performance of the bond strength of two-bottle bonding agent (Tokuyama Universal Bond II) was investigated under conditions without hydrofluoric acid solution (abbreviated as HF)-pretreatment of LDS. Methods: Nine resin cements (both self-adhesive and adhesive types) were used. It was investigated 1) the adhesion strength of various resin cements to LDS from the presence or absence of HF-treatment, 2) to determine the effect of the deterioration in three times [after one-day storage (abbreviated as Base), and after 5,000 & 20,000 thermocycles (abbreviated as TC 5k and TC 20k)] of one- and two-component bonding agents. And the difference in degradation between one- and two-component bonding gents consist of the silane coupling agent was performed by chemical analysis (High Performance Liquid Chromatography). Results: The trends of resin cements were statistically not very different for each cement 3 times with HF-conditions. Also ESTECEM II and Super-Bond Universal showed the significant greatest values in two conditions (TC 5k and TC 20k) without HF-condition. In TC 20k, ESTECEM II & Super-Bond Universal showed significantly better results than others when treated with the recommended bonding agents without HF-condition. In TC 20k, there was not much statistically significant difference if pretreated with Tokuyama Universal Bond II without HF-condition. Significance: When using LDS, it was found that long-term durability could be maintained by pretreating with Tokuyama Universal Bond II without pretreating with various hazardous HFs.

Keywords

Shear bond strength; bonding agent; one- vs. two bottles; resin luting materials; lithium disilicate ceramics; Durability 

Subject

Chemistry and Materials Science, Biomaterials

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