Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Improving Pure Titanium's Biological and Mechanical Characteristics through ECAP and Micro Arc Oxidation Processes

Version 1 : Received: 1 June 2023 / Approved: 2 June 2023 / Online: 2 June 2023 (10:01:53 CEST)

A peer-reviewed article of this Preprint also exists.

Alemayehu, D.B.; Todoh, M.; Hsieh, J.-H.; Li, C.; Huang, S.-J. Improving Pure Titanium’s Biological and Mechanical Characteristics through ECAP and Micro-Arc Oxidation Processes. Micromachines 2023, 14, 1541. Alemayehu, D.B.; Todoh, M.; Hsieh, J.-H.; Li, C.; Huang, S.-J. Improving Pure Titanium’s Biological and Mechanical Characteristics through ECAP and Micro-Arc Oxidation Processes. Micromachines 2023, 14, 1541.

Abstract

Pure titanium is limited to be used in biomedical applications due to its lower mechanical strength compared to its alloy counterpart. To enhance its properties and improve medical implants feasibility, advancements in titanium processing technologies are necessary. One such technique is equal channel angular pressing (ECAP) for its severe plastic deformation (SPD). This study aimed to surface modify commercially pure titanium using micro arc oxidation (MAO) technology and mineral solutions containing Ca and P. The composition and shape of the changed surface were characterized using X-ray diffraction (XRD) and scanning electron microscope (SEM), respectively. The weight % of Ca and P in the coating was determined using Energy Dispersive Spectroscopy (EDS), and the corrosion resistance was evaluated through potentiodynamic measurement. The behavior of human dental pulp cell and periodontal cell behavior was also studied through a biomedical experiment over a period of 1-, 3-, and 7-days using trypsin as the culture medium and ELISA as the observation method. This study showed that the mechanical grain refinement method and surface modification significantly improved the biomechanical properties of commercially pure (CP) Titanium. Although the results showed variations in the absorbance values of cells cultured on different surfaces, this study provides valuable insights into pulp cell behavior and advances the field of biomedical research.

Keywords

Pulp cell; Periodontal cell; Micro-Arc Oxidation (MAO), Sever Plastic deformation (SPD), Equal Channel Angular Pressing (ECAP), AlamarBlue; ELISA; trypsin

Subject

Engineering, Mechanical Engineering

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