Preprint Article Version 1 This version is not peer-reviewed

One-Step Fabrication of Composite Hydrophobic Electrically Heated Graphene Surface for Anti-Icing

Version 1 : Received: 30 June 2024 / Approved: 1 July 2024 / Online: 2 July 2024 (13:28:05 CEST)

How to cite: Zhong, M.; Li, S.; Fan, H.; Zhang, H.; Jiang, Y.; Luo, J.; Yang, L. One-Step Fabrication of Composite Hydrophobic Electrically Heated Graphene Surface for Anti-Icing. Preprints 2024, 2024070123. https://doi.org/10.20944/preprints202407.0123.v1 Zhong, M.; Li, S.; Fan, H.; Zhang, H.; Jiang, Y.; Luo, J.; Yang, L. One-Step Fabrication of Composite Hydrophobic Electrically Heated Graphene Surface for Anti-Icing. Preprints 2024, 2024070123. https://doi.org/10.20944/preprints202407.0123.v1

Abstract

Ice accumulation poses considerable challenges in transportation, notably in the domain of general aviation. The present study combines the strengths and limitations of conventional aircraft de-icing techniques with the emerging trend toward all-electric aircraft. The study aims to utilize laser-induced graphene (LIG) technology to create a multifunctional surface, seamlessly integrating hydrophobic properties with efficient electrical heating to mitigate surface icing effectively. We investigated the utilization of a 10.6 μm CO2 laser for direct writing on polyimide (PI), a widely-used insulating encapsulation material. From the thermomechanical perspective, our initial analysis using COMSOL Multiphysics software revealed that when the laser power P exceeds 5 W, the PI substrate experience ablative damage. The experimental results show that when P ≤ 5W, an increase in power has a positive impact on the quality, surface porosity, roughness reduction, line-spacing reduction, and water contact-angle enhancement of the graphene. Conversely, when P > 5 W, higher power negatively affects both the substrate and the graphene structure by inducing excessive ablation. However, it influences the graphene line height positively and is consistent with overall experimental-simulation congruence. Furthermore, the incorporation of high-quality graphene resulted in a surface that exhibited higher contact angles (CA > 120°), lower energy consumption, and higher heating efficiency compared to the use of traditional electrically heated materials for anti-icing applications. The potential applications of this one-step fabrication method extend across various industries, particularly aviation, marine engineering, and other ice-prone domains. Moreover, the method has extensive prospects for addressing pivotal challenges associated with ice formation and serves an innovative and efficient anti-icing technology.

Keywords

LIG; Hydrophobic surface; electrically heated materials; one-step fabrication; contact angle

Subject

Chemistry and Materials Science, Surfaces, Coatings and Films

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